Lookup NU author(s): Dr Xiao Han,
Professor Lidija Siller
This work is licensed under a Creative Commons Attribution 4.0 International License (CC BY 4.0).
Porous Zn-based and ZnO composites are successfully fabricated via the sol-gel process and ambient pressure drying (APD) method using hexane as the drying solvent for the reduction of capillary force during drying process. Various highly porous Zn-based phases (Zn1-based and Zn5-based) that are studied by X-ray diffraction analysis, scanning electron microscopy and transmission electron microscopy, show that they contribute through heat treatment (at 200°C) to the development of ambient pressure dried nanoporous wurtzite (hexagonal) ZnO. A macroporous flower-like structure consisting of nanosheets is observed in porous Zn-based composites and nanoporous structure is observed within platelets of ZnO nanoparticles. Possible routes for preparing highly porous Zn-based/ZnO composites are discovered by detailing the process for ambient pressure drying synthesis of porous wurzite ZnO.
Author(s): Han X, Harris J, Siller L
Publication type: Article
Publication status: Published
Journal: Journal of Materials Science
Print publication date: 01/06/2018
Online publication date: 26/02/2018
Acceptance date: 12/02/2018
Date deposited: 27/02/2018
ISSN (print): 0022-2461
ISSN (electronic): 1573-4803
Publisher: Springer New York LLC
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